![](/CAS/GIF/104227-71-6.gif)
(S)-3-Boc-Amino-gamma-butyrolactone synthesis
- Product Name:(S)-3-Boc-Amino-gamma-butyrolactone
- CAS Number:104227-71-6
- Molecular formula:C9H15NO4
- Molecular Weight:201.22
![Di-tert-butyl dicarbonate](/CAS/GIF/24424-99-5.gif)
24424-99-5
821 suppliers
$13.50/25G
![(S)-3-Boc-Amino-gamma-butyrolactone](/CAS/GIF/104227-71-6.gif)
104227-71-6
108 suppliers
$8.00/100mg
Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: AcCl
1.2: 100 percent / Et3N
2.1: 84 percent / Ph3P; hexachloroethane / CH2Cl2 / 2 h / 20 °C
3.1: 81 percent / LiBH4 / ethanol; tetrahydrofuran / 0 - 20 °C
4.1: 80 percent / Hunig's base / CH2Cl2 / 0 - 20 °C
5.1: HCl / methanol / 3 h / 20 °C
5.2: 65 percent Turnov. / CSA / benzene
References:
Kenworthy, Martin N.;Kilburn, John Paul;Taylor, Richard J. K. [Organic Letters,2004,vol. 6,# 1,p. 19 - 22]
![Di-tert-butyl dicarbonate](/CAS/GIF/24424-99-5.gif)
24424-99-5
821 suppliers
$13.50/25G
![Benzyl (S)-(-)-tetrahydro-5-oxo-3-furanylcarbamate](/CAS/GIF/87219-29-2.gif)
87219-29-2
129 suppliers
$7.00/100mg
![(S)-3-Boc-Amino-gamma-butyrolactone](/CAS/GIF/104227-71-6.gif)
104227-71-6
108 suppliers
$8.00/100mg
![5,7-Dioxa-2-aza-10-silaundecanoic acid, 3-(2-methoxy-2-oxoethyl)-10,10-dimethyl-, 1,1-dimethylethyl ester, (3S)-](/CAS/20210305/GIF/651036-65-6.gif)
651036-65-6
0 suppliers
inquiry
![(S)-3-Boc-Amino-gamma-butyrolactone](/CAS/GIF/104227-71-6.gif)
104227-71-6
108 suppliers
$8.00/100mg
![(S)-(-)-2-(Boc-Amino)-1,4-butanediol](/CAS/GIF/128427-10-1.gif)
128427-10-1
154 suppliers
$18.00/250mg
![(S)-(-)-alpha-(Boc-Amino)-gamma-butyrolactone](/CAS/GIF/40856-59-5.gif)
40856-59-5
127 suppliers
$7.00/250mg
![(S)-3-Boc-Amino-gamma-butyrolactone](/CAS/GIF/104227-71-6.gif)
104227-71-6
108 suppliers
$8.00/100mg
![Butanoic acid, 3-[[(1,1-diMethylethoxy)carbonyl]aMino]-4-hydroxy-, Methyl ester, (3S)-](/CAS/20150407/GIF/136703-59-8.gif)
136703-59-8
26 suppliers
inquiry
![(S)-3-Boc-Amino-gamma-butyrolactone](/CAS/GIF/104227-71-6.gif)
104227-71-6
108 suppliers
$8.00/100mg