tert-butyl 2-(4-hydroxyphenyl)acetate synthesis
- Product Name:tert-butyl 2-(4-hydroxyphenyl)acetate
- CAS Number:16010-88-1
- Molecular formula:C12H16O3
- Molecular Weight:208.25
![Zinc, bromo[2-(1,1-dimethylethoxy)-2-oxoethyl]-](/CAS/20180703/GIF/51656-70-3.gif)
Yield:16010-88-1 91%
Reaction Conditions:
Stage #1: 4-bromo-phenolwith potassium hydride in tetrahydrofuran at 20; for 0.166667 h;
Stage #2: (2-tert-butoxy-2-oxoethyl)zinc(II) bromidewith {[P(t-Bu)3]PdBr}2 in tetrahydrofuran at 20; for 4 h;
References:
Hama, Takuo;Liu, Xiaoxiang;Culkin, Darcy A.;Hartwig, John F. [Journal of the American Chemical Society,2003,vol. 125,# 37,p. 11176 - 11177]
![[p-(Benzyloxy)phenyl]acetic Acid tert-Butyl Ester](/CAS/20180703/GIF/19712-89-1.gif)
19712-89-1
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