![](/CAS/GIF/10581-12-1.gif)
Tetramethylammonium acetate synthesis
- Product Name:Tetramethylammonium acetate
- CAS Number:10581-12-1
- Molecular formula:C6H15NO2
- Molecular Weight:133.19
![Tetramethylammonium hydroxide](/CAS/GIF/75-59-2.gif)
75-59-2
373 suppliers
$12.00/25mL
![Acetic acid](/CAS/GIF/64-19-7.gif)
64-19-7
1536 suppliers
$10.00/25ML
![Tetramethylammonium acetate](/CAS/GIF/10581-12-1.gif)
10581-12-1
202 suppliers
$9.00/25g
Yield:10581-12-1 87.6%
Reaction Conditions:
in methanol at 40; for 4 h;
Steps:
[NMe4][Acetate] [12]; Used in CORM-349This is commercially available, but earliest reference found in [12].247 mg (4.11 mmol) of acetic acid and 1.50 g (4.11 mmol) of [NMe4][OH] (25 wt. % soln. in MeOH) were stirred in 10 ml of methanol for 4 hrs at 40° C. Following this, the solution was filtered and then the solvent removed on rotary evaporator to give a viscous oil, in which solid was starting to form. The last traces of solvent were removed under high vacuum to leave a white solid, which was washed with ether and then dried under vacuum.480 mg of a white solid were produced. Yield was 87.6%.
References:
Motterlini, Roberto Angelo;Mann, Brian Ernest;Scapens, David Alistair US2010/105770, 2010, A1 Location in patent:Page/Page column 12
![Ammonium acetate](/CAS/GIF/631-61-8.gif)
631-61-8
771 suppliers
$11.19/100G
![Dimethyl carbonate](/CAS/GIF/616-38-6.gif)
616-38-6
661 suppliers
$5.00/5 g
![Tetramethylammonium acetate](/CAS/GIF/10581-12-1.gif)
10581-12-1
202 suppliers
$9.00/25g
![Methanamine Acetate](/CAS/20180601/GIF/6998-30-7.gif)
6998-30-7
20 suppliers
$34.00/1G
![Dimethyl carbonate](/CAS/GIF/616-38-6.gif)
616-38-6
661 suppliers
$5.00/5 g
![Tetramethylammonium acetate](/CAS/GIF/10581-12-1.gif)
10581-12-1
202 suppliers
$9.00/25g