Trityl azide synthesis
- Product Name:Trityl azide
- CAS Number:14309-25-2
- Molecular formula:C19H15N3
- Molecular Weight:285.34
76-83-5
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14309-25-2
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Yield: 80%
Reaction Conditions:
in N-methyl-acetamide
Steps:
7.ii EXAMPLE 7 STR18
ii. 27.9 g (0.1 mole) of triphenylmethyl chloride were dissolved in 250 ml of dimethylformamide, 14 g (0.21 mole) of sodium azide were added to this solution and the mixture was stirred for 10 hours at 80° C. After this time, a further 8.5 g (0.16 mole) of sodium azide were added and the mixture was again stirred for 8 hours at 80° C. After filtering off the inorganic salt produced, there was left a dimethylformamide solution containing triphenylmethyl azide in approximately 80% yield.
References:
Bayer Aktiengesellschaft US4098894, 1978, A
76-84-6
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14309-25-2
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$190.00/5g
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14309-25-2
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14309-25-2
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100-58-3
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14309-25-2
78 suppliers
$190.00/5g