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ChemicalBook CAS DataBase List 3-CHLORO-4-HYDROXYACETANILIDE

3-CHLORO-4-HYDROXYACETANILIDE synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 89 percent / 4-dimethylaminopyridine, pyridine / diethyl ether; dioxane / 5 h / Ambient temperature
2: AlCl3, PhCH2SH / CH2Cl2 / 1) 0 deg C, 2) r.t., 3 h

References:

Kuehm-Caubere, Catherine;Caubere, Paul;Jamart-Gregoire, Brigitte;Pfeiffer, Bruno;Guardiola-Lemaitre, Beatrice;Manechez, Dominique;Renard, Pierre [European Journal of Medicinal Chemistry,1999,vol. 34,# 1,p. 51 - 61]

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