1,3-Adamantanediamine
![1,3-Adamantanediamine Structure](CAS/GIF/10303-95-4.gif)
- CAS No.
- 10303-95-4
- Chemical Name:
- 1,3-Adamantanediamine
- Synonyms
- 13AD;1,3-Adamantanediamine;1,3-Diaminoadamantane;1, 3-Amantadane Diamine;4. 1,3-diaminoadamantane;Adamantan-1,3-diyldiamin;10303-95-4 1,3-Adamantanediamine;1,3-Adamantanediaminewith2HClsalt;Benzeneethanol,5-amino-β,β-dimethyl-;Tricyclo[3.3.1.13,7]decane-1,3-diamine
- CBNumber:
- CB11030056
- Molecular Formula:
- C10H18N2
- Molecular Weight:
- 166.26
- MOL File:
- 10303-95-4.mol
- MSDS File:
- SDS
- Modify Date:
- 2023/6/8 17:06:37
Boiling point | 249 °C |
---|---|
Density | 1.153 |
Flash point | 122 °C |
pka | 10.73±0.40(Predicted) |
form | powder to crystal |
color | White to Almost white |
CAS DataBase Reference | 10303-95-4(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | ![]() GHS05 |
|||||||||
---|---|---|---|---|---|---|---|---|---|---|
Signal word | Danger | |||||||||
Hazard statements | H314 | |||||||||
Precautionary statements | P501-P260-P264-P280-P303+P361+P353-P301+P330+P331-P363-P304+P340+P310-P305+P351+P338+P310-P405 | |||||||||
HS Code | 2921.30.5000 | |||||||||
NFPA 704 |
|
1,3-Adamantanediamine price More Price(2)
1,3-Adamantanediamine Chemical Properties,Uses,Production
Preparation
1,3-Adamantanediamine synthesis: 1,3-Adamantane dicarboxylic acid (12 g) was mixed with 50 mL of SOCl2 and the mixture was refluxed for 3 h. Excessive SOCl2 was evaporated and 1,3-adamantane dicarbonyl dichloride was obtained as white solid, dissolved in dried benzene and added to cold ammonia solution slowly, during which a white precipitate was formed gradually filtered and then washed the precipitate several times with water to give 1,3-disaminoacyladamantane as white solid, recrystallized from ethanol. White solid, yield 10.58 g (89 %).
Purification Methods
Purify it by zone refining. The dibenzoyl derivative has m 248o, and the dihydrochloride salt has m 310o (360o) after recrystallisation from aqueous EtOH or EtOH/Et2O. [Prelog & Seiwerth Chem Ber 74 1769 1941, Stetter & Wulff Chem Ber 93 1366 1960.]
1,3-Adamantanediamine Preparation Products And Raw materials
Raw materials
Preparation Products
Supplier | Tel | Country | ProdList | Advantage | Inquiry |
---|---|---|---|---|---|
TCI Chemicals (India) Pvt. Ltd. | 1800 425 7889 | New Delhi, India | 6778 | 58 | Inquiry |
Pharmaffiliates Analytics and Synthetics P. Ltd | +91-172-5066494 | Haryana, India | 6773 | 58 | Inquiry |
A.J Chemicals | 91-9810153283 | New Delhi, India | 6124 | 58 | Inquiry |
Shanghai Qyubiotech Co., Ltd. | +86-086-021-37596619 +8618019359838 | China | 300 | 58 | Inquiry |
Capot Chemical Co.,Ltd. | 571-85586718 +8613336195806 | China | 29798 | 60 | Inquiry |
Shanghai Daken Advanced Materials Co.,Ltd | +86-371-66670886 | China | 18646 | 58 | Inquiry |
Henan Tianfu Chemical Co.,Ltd. | +86-0371-55170693 +86-19937530512 | China | 21667 | 55 | Inquiry |
career henan chemical co | +86-0371-86658258 +8613203830695 | China | 29888 | 58 | Inquiry |
Chongqing Chemdad Co., Ltd | +86-023-6139-8061 +86-86-13650506873 | China | 39916 | 58 | Inquiry |
SIMAGCHEM CORP | +86-13806087780 | China | 17367 | 58 | Inquiry |