2-Chloro-1,3-dinitrobenzene

2-Chloro-1,3-dinitrobenzene Structure
CAS No.
606-21-3
Chemical Name:
2-Chloro-1,3-dinitrobenzene
Synonyms
2,6-DINITROCHLOROBENZENE;Bendamustine Impurity 53;Vortioxetine Impurity 65;2,6-Dinitrophenyl chloride;2-Chloro-1,3-dintrobenzene;2-CHLORO-1,3-DINITROBENZENE;2-chloro-1,3-dinitro-benzen;1,3-Dinitro-2-chlorobenzene;1-CHLORO-2,6-DINITROBENZENE;2,6-Dinitro-1-Chlorobenzene
CBNumber:
CB2340629
Molecular Formula:
C6H3ClN2O4
Molecular Weight:
202.55
MOL File:
606-21-3.mol
MSDS File:
SDS
Modify Date:
2023/4/23 13:52:06

2-Chloro-1,3-dinitrobenzene Properties

Melting point 86-88°C
Boiling point 315°C
Density 1,687 g/cm3
refractive index 1.5870 (estimate)
Flash point 315°C
storage temp. 2-8°C
form solid
color Pale-yellow to Yellow-brown
Water Solubility Soluble in alcohol. Moderately soluble in benzene, ether. Practically insoluble in water.
Merck 14,2137
BRN 522187
CAS DataBase Reference 606-21-3(CAS DataBase Reference)
NIST Chemistry Reference 1-Chloro-2,6-dinitrobenzene(606-21-3)
EPA Substance Registry System 2,6-Dinitrochlorobenzene (606-21-3)

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS06,GHS08,GHS09
Signal word  Danger
Hazard statements  H300-H310-H330-H373-H400-H410
Precautionary statements  P301+P310a-P304+P340-P320-P330-P405-P501a
Risk Statements  23/24/25-33-50/53
Safety Statements  28-36/37-45-60-61
RIDADR  3441
RTECS  CZ0525500
TSCA  Yes
HazardClass  6.1
PackingGroup  II
HS Code  29049090
NFPA 704
1
4 0

2-Chloro-1,3-dinitrobenzene price More Price(2)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
ALFA India ALF-L04593-06 2-Chloro-1,3-dinitrobenzene, 98+% 606-21-3 5g ₹16496 2022-05-26 Buy
ALFA India ALF-L04593-03 2-Chloro-1,3-dinitrobenzene, 98+% 606-21-3 1g ₹4447 2022-05-26 Buy
Product number Packaging Price Buy
ALF-L04593-06 5g ₹16496 Buy
ALF-L04593-03 1g ₹4447 Buy

2-Chloro-1,3-dinitrobenzene Chemical Properties,Uses,Production

Chemical Properties

Yellow crystals. Soluble in ethanol, ether, and toluene

Uses

2-Chloro-1,3-dinitrobenzene can be used as intermediates of dyes and pigments. Also used as solvents in HPLC, NMR.

Uses

2,6-Dinitrochlorobenzene (2-Chloro-1,3-dinitrobenzene) is a thiol-modifying agent.

Hazard

Toxic if swallowed. Toxic in contact with skin. Fatal if inhaled. May cause damage to organs through prolonged or repeated exposure. Very toxic to aquatic life with long lasting effects.

Synthesis

The synthesis of 2-Chloro-1,3-dinitrobenzene is as follows:
Add 800ml of sulfolane as solvent to a 2L flask, then add 246.5g of 3,5-dinitro-4-chlorobenzoic acid and 168g of sodium bicarbonate,Heat to 195°C to react for 2h. After the reaction is complete, cool to 130°C and distill under reduced pressure.The product 2-Chloro-1,3-dinitrobenzene, 178.4g, was obtained by rectification with a yield of 88.1%.
synthesis of 2-Chloro-1,3-dinitrobenzene.png

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2-Chloro-1,3-dinitrobenzene Spectrum

1-CHLORO-2,6-DINITROBENZENE 1,3-Dinitro-2-chlorobenzene 2-chloro-1,3-dinitro-benzen 2-Chloro-1,3-dintrobenzene 2,6-Dinitrophenyl chloride 2,6-Dinitro-1-Chlorobenzene Benzene, 2-chloro-1,3-dinitro- 1-Chloro-2,6-dinitrobenzene~2,6-Dinitrochlorobenzene 2,6-DINITROCHLOROBENZENE 2-CHLORO-1,3-DINITROBENZENE 2-Chloro-1,3-dinitrobenzene, 98+% Bendamustine Impurity 53 606-21-3 2-Chloro-1,3-dinitrobenzene Vortioxetine Impurity 65 606-21-3 NO22ClC6H3 Intermediates of Dyes and Pigments Alcohols and Derivatives