(R)-1-BOC-3-(ヒドロキシメチル)ピペラジン
(R)-1-BOC-3-(ヒドロキシメチル)ピペラジン 物理性質
- 融点 :
- 68-70°C
- 沸点 :
- 322.9±22.0 °C(Predicted)
- 比重(密度) :
- 1.085±0.06 g/cm3(Predicted)
- 貯蔵温度 :
- Keep in dark place,Sealed in dry,Room Temperature
- 溶解性:
- クロロホルム（微量）、メタノール（微量）
- 外見 :
- 個体
- 酸解離定数(Pka):
- 14.97±0.10(Predicted)
- 色:
- ホワイトからオフホワイト
- InChI:
- InChI=1S/C10H20N2O3/c1-10(2,3)15-9(14)12-5-4-11-8(6-12)7-13/h8,11,13H,4-7H2,1-3H3/t8-/m1/s1
- InChIKey:
- NSILYQWHARROMG-MRVPVSSYSA-N
- SMILES:
- N1(C(OC(C)(C)C)=O)CCN[C@@H](CO)C1
- CAS データベース:
- 278788-66-2(CAS DataBase Reference)
(R)-1-BOC-3-(ヒドロキシメチル)ピペラジン 価格
もっと(15)
| メーカー |
製品番号 |
製品説明 |
CAS番号 |
包装 |
価格 |
更新時間 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01MAS070016 |
(R)-1-Boc-3-(ヒドロキシメチル)ピペラジン
(R)-1-Boc-3-(Hydroxymethyl)piperazine |
278788-66-2 |
25g |
￥455400 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOOR308071 |
(3R)-3-(Hydroxymethyl)piperazine, N1-BOC protected |
278788-66-2 |
1g |
￥5800 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01APOOR308071 |
(3R)-3-(Hydroxymethyl)piperazine, N1-BOC protected |
278788-66-2 |
5g |
￥43200 |
2023-06-01 |
購入 |
|
Sigma-Aldrich Japan
|
SYX00408 |
(R)-1-BOC-3-(Hydroxymethyl)piperazine |
278788-66-2 |
1g |
￥87500 |
2024-03-01 |
購入 |
|
富士フイルム和光純薬株式会社(wako)
|
W01MAS070016 |
(R)-1-Boc-3-(ヒドロキシメチル)ピペラジン
(R)-1-Boc-3-(Hydroxymethyl)piperazine |
278788-66-2 |
1g |
￥45100 |
2024-03-01 |
購入 |
(R)-1-BOC-3-(ヒドロキシメチル)ピペラジン 化学特性,用途語,生産方法
合成
1,4-bis-Boc-2-hydroxymethylpiperazine (13.9 kg) and 95% ethanol (30 kg) were added to the reactor, followed by the addition of an aqueous solution (water 21 kg) of configured sodium hydroxide (3.5 kg). The reaction mixture was then heated to reflux. Once the reaction was completed, ethanol was concentrated under reduced pressure. Subsequently, 30 kg of dichloromethane was added and the mixture was separated into liquid and aqueous phases. The aqueous phase was extracted three times with 3 × 20 kg of dichloromethane, and the organic phases were combined. The resulting solution was washed once with 40 kg of a 15% aqueous sodium chloride solution and dried with anhydrous sodium sulfate. Further purification was carried out to obtain (R)-1-BOC-3-(Hydroxymethyl)piperazine.
(R)-1-BOC-3-(ヒドロキシメチル)ピペラジン 上流と下流の製品情報
原材料
準備製品
(R)-1-BOC-3-(ヒドロキシメチル)ピペラジン 生産企業
Global( 246)Suppliers
(R)-1-BOC-3-(ヒドロキシメチル)ピペラジン スペクトルデータ(1HNMR、FT-IR)
278788-66-2((R)-1-BOC-3-(ヒドロキシメチル)ピペラジン)キーワード:
- 278788-66-2
- (R)-3-HYDROXYMETHYL-PIPERAZINE-1-CARBOXYLIC ACID TERT-BUTYL ESTER
- (R)-4-N-BOC-2-HYDROXYMETHYL-PIPERAZINE
- (R)-1-Boc-3-hydroxymethyl-piperazine
- H57159
- (R)-4-Boc-2-hydroxymethyl-piperazine
- 1-Piperazinecarboxylic acid, 3-(hydroxymethyl)-, 1,1-dimethylethyl ester, (3R)-
- (R)-1-Boc-3-(Hydroxymethyl)piperazine ,98%
- (R)-4-N-Boc-2-hydroxyMeth...
- (R)-1-Boc-3-(hyroxyMethyl)piperazine
- (3R)-3-(Hydroxymethyl)piperazine, N1-BOC protected
- tert-Butyl (3R)-3-(hydroxymethyl)piperazine-1-carboxylate, (3R)-1-(tert-Butoxycarbonyl)-3-(hydroxymethyl)piperazine
- (3R)-1-Boc-3-(hydroxyMethyl)-piperazine
- (3R)-3-(Hydroxymethyl)piperazine, N1-BOC protected 98%
- (3R)-3-(hydroxymethyL
- (3R)-3-(Hydroxymethyl)piperazine
- ert-butyl(3R)-3-(hydroxymethyl)piperazine-1-carboxylate
- (R)-tert-Butyl 3-(hydroxymethyl)piperazine-1-carboxylate
- tert-butyl (3R)-3-(hydroxymethyl)piperazine-1-carboxylate
- tert-butyl (R)-3-(hydroxymethyl)piperazine-1-carboxylate
- tert-Butyl (3R)-3-(hydroxymethyl)-1-piperazinecarboxylate
- PIPERAZINE-1-CARBOXYLIC
- (3R)-3-(hydroxymethyl)-1-Piperazinecarboxylic acid tert-butyl ester
- (R)-1-BOC-3-(ヒドロキシメチル)ピペラジン