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3,5-Lutidine

3,5-Lutidine

CAS:
591-22-0
MF:
C7H9N
MW:
107.15

Properties

Melting point:
?9 °C (lit.)
Boiling point:
169-170 °C (lit.)
Density 
0.939 g/mL at 25 °C (lit.)
vapor pressure 
1.5 mm Hg ( 20 °C)
refractive index 
n20/D 1.504(lit.)
Flash point:
128 °F
storage temp. 
2-8°C
form 
Liquid
pka
6.15(at 25℃)
color 
Clear yellow
Water Solubility 
33 g/L (20 ºC)
Sensitive 
Hygroscopic
BRN 
105682
InChIKey
HWWYDZCSSYKIAD-UHFFFAOYSA-N
LogP
1.780

Safety Information

Symbol(GHS) 

GHS02,GHS05,GHS06
Signal word 
Danger
Hazard statements 
H226-H302-H311+H331-H314
Precautionary statements 
P210-P280-P301+P312-P303+P361+P353-P304+P340+P310-P305+P351+P338
Hazard Codes 
Xn,F,Xi,T
Risk Statements 
10-20/21/22-36/37/38-41-34-23/25-21
Safety Statements 
16-26-36-36/37-45-36/37/39
RIDADR 
UN 1993 3/PG 3
WGK Germany 
3
8
Hazard Note 
Irritant/Flammable
TSCA 
Yes
HazardClass 
3
PackingGroup 
III
HS Code 
29333999

Use

Dry 3,5-lutidine with sodium and fractionally distil it through a Todd column (p 11) packed with glass helices. Dissolve (100mL) in dilute HCl (1:4) and steam distil this until 1L of distillate is collected. Excess conc NaOH is added to the residue which is again steam distilled. The base is extracted from the distillate, using diethyl ether. The extract is dried over K2CO3, and distilled. It is then fractionally crystallised by partial freezing. The hydrochloride has m 229o(sublimes at 190-231o), and the picrate has m 242-243o(dec, from H2O), 249-250o(dec, from AcOH). [Beilstein 20 II 161, 20 III/IV 2788, 20/6 V 60.]

38 India supplier list of "3,5-Lutidine "

  • Product Name:3,5-Lutidine, 98%
  • Products Intro:Purity: 99% | Package: 1 kg,5 kg, 10 kg,25kg and 1 MT
  • Company Type: Trader
  • Country/Region: Gujarat,INDIA
  • Product Name:3,5-Lutidine
  • Products Intro:Purity: 98% | Package: 1 kg,5 kg, 10 kg,25kg and 1 MT
  • Company Type: Reagent
  • Country/Region: Uttar Pradesh,INDIA
  • Product Name:3,5-Lutidine
  • Products Intro:Purity: 98% | Package: 1 kg,5 kg, 10 kg,25kg and 1 MT
  • Company Type: Reagent
  • Country/Region: Maharashtra,INDIA
  • Product Name:3,5-Lutidine
  • Products Intro:Purity: 99% | Package: 1 kg,5 kg, 10 kg,25kg and 1 MT
  • Company Type: Manufacturer
  • Country/Region: Telangana,INDIA
  • Product Name:3,5-Lutidine
  • Products Intro:Purity: 98% | Package: 1 kg,5 kg, 10 kg,25kg and 1 MT
  • Company Type: Manufacturer
  • Country/Region: Maharashtra,INDIA
  • Product Name:3,5-Lutidine
  • Products Intro:Brand:sigma aldrich | Product Number:L4206 | Purity:≥98%
  • Company Type: Trader
  • Country/Region: Bangalore,INDIA
  • Product Name:3,5-Lutidine
  • Company Type: Trader
  • Country/Region: New Delhi,INDIA
  • Product Name:3,5-Lutidine
  • Company Type: Trader
  • Country/Region: New Delhi,INDIA
  • Product Name:3,5-Lutidine
  • Company Type: Trader
  • Country/Region: New Delhi,INDIA
  • Product Name:3,5-Lutidine
  • Company Type: Trader
  • Country/Region: New Delhi,INDIA

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