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apomorphine
apomorphine
- CAS:
- 58-00-4
- MF:
- C17H17NO2
- MW:
- 267.32
Properties
- Melting point:
- 195°C (rough estimate)
- Boiling point:
- 410.51°C (rough estimate)
- Density
- 1.0690 (rough estimate)
- refractive index
- 1.5400 (estimate)
- solubility
- Aqueous Base (Slightly), DMSO (Slightly)
- pka
- 7.0, 8.92(at 25℃)
- form
- Solid
- color
- White, crystalline alkaloid
- Water Solubility
- 20g/L(25 ºC)
- Stability:
- Hygroscopic
Safety Information
- Toxicity
- LD50 oral in mouse: > 100mg/kg
Use
Crystallise R-apomorphine from CHCl3 and a little pet ether, also from Et2O with 1 mol of Et2O which it loses at 100o. It sublimes in a high vacuum. It is white but turns green in moist air or in alkaline solution. UV: max 336, 399 (98% EtOH). The di-O-methylether is an oil b 175o/high vacuum, whose picrate crystallises from MeOH and has m 140o (dec). The di-O-acetate crystallises from EtOAc/pet ether with m 127-128o, [] D -88o (c 1, 0.1 N HCl). The di-O-benzoyl derivative has m 156-158o (from EtOH) and []D +43.44o (c 3.3, CHCl3). [Pachorr et al. Chem Ber 35 4377 1902, Beilstein 21 H 246.] NARCOTIC.
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