ChemicalBook CAS DataBase List 4-(4-Aminophenyl)-3-methyl-4-oxobutanoic acid

4-(4-Aminophenyl)-3-methyl-4-oxobutanoic acid synthesis

3synthesis methods

Product Name:4-(4-Aminophenyl)-3-methyl-4-oxobutanoic acid
CAS Number:42075-29-6
Molecular formula:C11H13NO3
Molecular Weight:207.23

62-23-7 Synthesis

62-23-7
679 suppliers
$14.00/25g

4-(4-Aminophenyl)-3-methyl-4-oxobutanoic acid

42075-29-6
76 suppliers
$11.00/250mg

Yield:-

Steps:

Multi-step reaction with 6 steps
1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 34 h / 26 °C / Large scale
2: sodium ethanolate / N,N-dimethyl-formamide / 15.5 h / -5 - 0 °C / Large scale
3: ethanol / 16 h / 52 °C / Large scale
4: sodium ethanolate / N,N-dimethyl-formamide / 14 h / 16 °C / Large scale
5: sodium hydroxide / ethanol / 28 h / 67 °C / Large scale
6: hydrogen / ethanol / 22 h / 58 °C / 1520.1 Torr / Large scale

References:

AstaTech (Chengdu) Biopharmaceutical Co., Ltd;WEI, GENGHUI;LIU, WEIGUO;LUO, JIANYE;GUO, PENG CN104496834, 2016, B

4-(4-Aminophenyl)-3-methyl-4-oxobutanoic acid Related Search:

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