![](/CAS/GIF/2051-62-9.gif)
4-Chlorobiphenyl synthesis
- Product Name:4-Chlorobiphenyl
- CAS Number:2051-62-9
- Molecular formula:C12H9Cl
- Molecular Weight:188.65
![1,4-Dichlorobenzene](/CAS/GIF/106-46-7.gif)
106-46-7
501 suppliers
$10.00/5g
![PHENYLMAGNESIUM BROMIDE](/CAS/GIF/100-58-3.gif)
100-58-3
185 suppliers
$18.00/10ml
![4-Chlorobiphenyl](/CAS/GIF/2051-62-9.gif)
2051-62-9
133 suppliers
$35.00/250mg
Yield:2051-62-9 91.3%
Reaction Conditions:
with Ni(N,N'-bis(diphenylphosphino)-1,3-benzenediamine(-1H))Cl in tetrahydrofuran at 40; for 18 h;Schlenk technique;Inert atmosphere;Kumada Cross-Coupling;
Steps:
2.3. Typical procedure for the Kumada coupling reaction
General procedure: Aryl chloride (1.0 mmol), ArMgBr (1.5 mmol) in THF (2.0 mL), catalysts (2.0 mol%), were added to a Schlenk tube under an N2 atmosphere. The reaction was stirred at 40 °C for 12 h.
References:
Sun, Yunqiang;Li, Xiaoyan;Sun, Hongjian [Inorganica Chimica Acta,2014,vol. 415,p. 95 - 97]
![1,4-Dichlorobenzene](/CAS/GIF/106-46-7.gif)
106-46-7
501 suppliers
$10.00/5g
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98-80-6
714 suppliers
$5.00/5g
![4-Chlorobiphenyl](/CAS/GIF/2051-62-9.gif)
2051-62-9
133 suppliers
$35.00/250mg
![4-Bromochlorobenzene](/CAS/GIF/106-39-8.gif)
106-39-8
444 suppliers
$14.00/5g
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780-69-8
308 suppliers
$9.00/25g
![4-Chlorobiphenyl](/CAS/GIF/2051-62-9.gif)
2051-62-9
133 suppliers
$35.00/250mg
![4-Bromochlorobenzene](/CAS/GIF/106-39-8.gif)
106-39-8
444 suppliers
$14.00/5g
![TRIBUTYLPHENYLTIN](/CAS/GIF/960-16-7.gif)
960-16-7
94 suppliers
$22.60/1g
![4-Chlorobiphenyl](/CAS/GIF/2051-62-9.gif)
2051-62-9
133 suppliers
$35.00/250mg
![4-Bromochlorobenzene](/CAS/GIF/106-39-8.gif)
106-39-8
444 suppliers
$14.00/5g
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591-51-5
127 suppliers
$45.89/50ml
![4-Chlorobiphenyl](/CAS/GIF/2051-62-9.gif)
2051-62-9
133 suppliers
$35.00/250mg