![](/CAS/GIF/577-72-0.gif)
4-METHOXY-3-NITROANILINE synthesis
- Product Name:4-METHOXY-3-NITROANILINE
- CAS Number:577-72-0
- Molecular formula:C7H8N2O3
- Molecular Weight:168.15
![1-Methoxy-2,4-dinitrobenzene](/CAS/GIF/119-27-7.gif)
119-27-7
2 suppliers
$658.00/2500g
![4-METHOXY-3-NITROANILINE](/CAS/GIF/577-72-0.gif)
577-72-0
144 suppliers
$45.00/50mg
Yield:577-72-0 98.1%
Reaction Conditions:
with PdCu/graphene double-metal catalyst at 60; under 7500.75 Torr; for 0.583333 h;Pressure;Time;Reagent/catalyst;
Steps:
7
The prepared 2,4-dinitroanisole (II) was dissolved in 2 kg of methanol solution, followed by the addition of 60 g of Example 1PdCu / graphene bimetallic catalyst prepared by catalytic hydrogenation reduction reaction,Reaction pressure is 1Mpa,Reaction temperature is 60 ,Reaction time 35min,The reaction is over.After the filter to remove the catalyst,Distillation recovery of methanol,Washed,749.26 g of 4-amino-2-nitroanisole (III) (HPLC purity 99.6%) was obtained,Yield 98.1%.
References:
CN107673976,2018,A Location in patent:Paragraph 0059-0060; 0072; 0081
![N-(4-METHOXY-3-NITROPHENYL)ACETAMIDE](/CAS/GIF/50651-39-3.gif)
50651-39-3
40 suppliers
inquiry
![4-METHOXY-3-NITROANILINE](/CAS/GIF/577-72-0.gif)
577-72-0
144 suppliers
$45.00/50mg
![p-Anisidine](/CAS/GIF/104-94-9.gif)
104-94-9
474 suppliers
$9.00/1g
![4-METHOXY-3-NITROANILINE](/CAS/GIF/577-72-0.gif)
577-72-0
144 suppliers
$45.00/50mg
![4-Amino-2-nitrophenol](/CAS/GIF/119-34-6.gif)
119-34-6
146 suppliers
$18.00/5g
![Iodomethane](/CAS/GIF/74-88-4.gif)
74-88-4
340 suppliers
$15.00/10g
![4-METHOXY-3-NITROANILINE](/CAS/GIF/577-72-0.gif)
577-72-0
144 suppliers
$45.00/50mg
![1-Methoxy-2,4-dinitrobenzene](/CAS/GIF/119-27-7.gif)
119-27-7
2 suppliers
$658.00/2500g
![4-METHOXY-3-NITROANILINE](/CAS/GIF/577-72-0.gif)
577-72-0
144 suppliers
$45.00/50mg
![2-Amino-4-nitro anisidine](/CAS/GIF/99-59-2.gif)
99-59-2
202 suppliers
$15.00/5mg