Benzonitrile, 2-fluoro-3-methoxy- (9CI) synthesis
- Product Name:Benzonitrile, 2-fluoro-3-methoxy- (9CI)
- CAS Number:198203-94-0
- Molecular formula:C8H6FNO
- Molecular Weight:151.14
321-28-8
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198203-94-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: N,N,N',N'',N'''-pentamethyldiethylenetriamine; n-butyllithium / hexane; tetrahydrofuran / 2.5 h / -78 - -70 °C
2.1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 4 h / 20 °C
2.2: 2 h / 0 - 20 °C
3.1: trifluoromethylsulfonic anhydride; pyridine / dichloromethane / 16 h / -60 - 20 °C
References:
Deichert, Julie A.;Mizufune, Hideya;Patel, Jignesh J.;Hurst, Timothy E.;Maheta, Ashish;Kitching, Matthew O.;Ross, Avena C.;Snieckus, Victor [European Journal of Organic Chemistry,2020,vol. 2020,# 30,p. 4693 - 4697]
198204-64-7
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198203-94-0
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137654-20-7
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198203-94-0
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