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ChemicalBook CAS DataBase List BENZOYL BROMIDE

BENZOYL BROMIDE synthesis

11synthesis methods
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Yield:-

Reaction Conditions:

with lithium bromide at 75; for 4 h;Inert atmosphere;

Steps:

2.2. Synthesis of Cs3Bi2Br9 Double Perovskite
1. Conversion of benzoyl chloride into benzoyl bromide:The reaction was performed in N2 atmosphere. 2 mL ofbenzoyl chloride was added to 1.7369 g of LiBr in 25 mLthree nick flask. The flak was kept on a hot plate at 75 °C for 4 h and the mixture was continuously stirred. The mixture converts from colourless to orange colour, indicating formation of benzoyl bromide. It was cooled down to room temperature (RT) and filtered using a PTFE membranewith 0.45 m pore size [15].

References:

Kumar, Ashish;Rawat, S. S.;Singh, Vidya Nand;Srivastava, Ritu;Swami, Sanjay Kumar [Journal of Nanoscience and Nanotechnology,2020,vol. 20,# 6,p. 3802 - 3808]

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