L-Lactide synthesis
- Product Name:L-Lactide
- CAS Number:4511-42-6
- Molecular formula:C6H8O4
- Molecular Weight:144.13
79-33-4
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4511-42-6
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Yield:4511-42-6 94%
Reaction Conditions:
in water at 240; under 760.051 Torr;Inert atmosphere;Autoclave;
Steps:
3 3. Catalytic reaction
The catalytic reaction was carried out after loading 1 g of catalyst into a conventional stainless steel fixed bed reactor (inner diameter 5 mm, length 300 mm). Next, the 75%water-receiving LA was vaporized in the pre-heating line and mixed with N2 beforeintroduction into the reactor via the liquid pump. The product was recovered from thereactor through a heating line into a sample vessel maintained at 5 ° C, at which thecrude droplet and unreacted LA were separated into a crystalline phase and a liquid phase, respectively.
References:
KR2018/103267,2018,A Location in patent:Paragraph 0096; 0097; 0104; 0107; 0112
687-47-8
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4511-42-6
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97-62-1
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4511-42-6
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