ChemicalBook CAS DataBase List Tributyltin azide

Tributyltin azide synthesis

5synthesis methods

Product Name:Tributyltin azide
CAS Number:17846-68-3
Molecular formula:C12H27N3Sn
Molecular Weight:332.07

A cooled solution of sodium azide (4.10 g, 63.0 mmol) in water (13 mt) at 8°C BusSnCI (17 1 ml) is added dropwise while stirring the solution. After 2h of stirring at 8°C, dichloromethane (38 mi) is added, stirred for another 5 minutes, and phases separated. The water phase is washed with dichloromethane (13 ml). Combined organic phases are washed with 10% NaCI (13 ml) and distilled water (13 ml). The organic phase is dried with sodium sulfate (6.34 g), and the solvent is removed under reduced pressure to give the oily product Tributyltin azide (19.2 g, 91.8%).

56-35-9 Synthesis

56-35-9
194 suppliers
$30.00/100 g

17846-68-3
114 suppliers
$19.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps

References:

[Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56]

1461-22-9
219 suppliers
$10.00/10g

17846-68-3
114 suppliers
$19.00/1g

References

4648-54-8
310 suppliers
$16.80/5G

1461-22-9
219 suppliers
$10.00/10g

17846-68-3
114 suppliers
$19.00/1g

References

938-10-3 Synthesis

938-10-3
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1067-52-3 Synthesis

1067-52-3
94 suppliers
$49.20/25g

17846-68-3
114 suppliers
$19.00/1g

References

1067-24-9
11 suppliers
inquiry

17846-68-3
114 suppliers
$19.00/1g

References

Tributyltin azide Related Search:

Tributyl phosphate Tetrabutylammonium azide Trityl azide Triisopropylsilyl chloride Azide

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