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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List Tributyltin azide
17846-68-3

Tributyltin azide synthesis

5synthesis methods
A cooled solution of sodium azide (4.10 g, 63.0 mmol) in water (13 mt) at 8°C BusSnCI (17 1 ml) is added dropwise while stirring the solution. After 2h of stirring at 8°C, dichloromethane (38 mi) is added, stirred for another 5 minutes, and phases separated. The water phase is washed with dichloromethane (13 ml). Combined organic phases are washed with 10% NaCI (13 ml) and distilled water (13 ml). The organic phase is dried with sodium sulfate (6.34 g), and the solvent is removed under reduced pressure to give the oily product Tributyltin azide (19.2 g, 91.8%).
Tributyltin azide
56-35-9 Synthesis
Bis(tributyltin) oxide

56-35-9
185 suppliers
$30.00/100 g

Tributyltin azide

17846-68-3
109 suppliers
$19.00/1g

-

Yield:-

Steps:

Multi-step reaction with 2 steps

References:

[Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.1, page 38 - 56]

Tributyltin chloride

1461-22-9
212 suppliers
$10.00/10g

Tributyltin azide

17846-68-3
109 suppliers
$19.00/1g

References
Azidotrimethylsilane

4648-54-8
301 suppliers
$16.80/5G

Tributyltin chloride

1461-22-9
212 suppliers
$10.00/10g

Tributyltin azide

17846-68-3
109 suppliers
$19.00/1g

References
938-10-3 Synthesis
Benzenesulfonylazide

938-10-3
12 suppliers
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1067-52-3 Synthesis
TRI-N-BUTYLTIN METHOXIDE

1067-52-3
92 suppliers
$49.20/25g

Tributyltin azide

17846-68-3
109 suppliers
$19.00/1g

References
DIMETHYLAMINOTRI-N-BUTYLTIN

1067-24-9
12 suppliers
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Tributyltin azide

17846-68-3
109 suppliers
$19.00/1g

References

Tributyltin azide Related Search:

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