5-Methoxyindole
- CAS No.
- 1006-94-6
- Chemical Name:
- 5-Methoxyindole
- Synonyms
- 5-METHOXY-1H-INDOLE;Methoxyindole 99% indol-5-yl methyl ether;5-methoxy-indol;Femedol;NSC 521752;AKOS JY2082918;5-METHOXYINDOLE;methoxy-5indole;5-MethoxyindoleF;Methoxy-5 indole
- CBNumber:
- CB4223553
- Molecular Formula:
- C9H9NO
- Molecular Weight:
- 147.17
- MOL File:
- 1006-94-6.mol
- MSDS File:
- SDS
- Modify Date:
- 2024/7/24 17:31:20
| Melting point | 52-55 °C (lit.) |
|---|---|
| Boiling point | 176-178 °C/17 mmHg (lit.) |
| Density | 1.1135 (rough estimate) |
| refractive index | 1.5310 (estimate) |
| Flash point | 176-178°C/17mm |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| solubility | Chloroform, Methanol |
| form | Crystalline Powder |
| pka | 16.70±0.30(Predicted) |
| color | White to light brownish |
| Water Solubility | insoluble |
| Sensitive | Light Sensitive |
| BRN | 116722 |
| InChIKey | DWAQDRSOVMLGRQ-UHFFFAOYSA-N |
| CAS DataBase Reference | 1006-94-6(CAS DataBase Reference) |
| NIST Chemistry Reference | 1H-Indole, 5-methoxy-(1006-94-6) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H315-H319-H335 | |||||||||
| Precautionary statements | P261-P264-P271-P280-P302+P352-P305+P351+P338 | |||||||||
| Hazard Codes | Xi | |||||||||
| Risk Statements | 36/37/38 | |||||||||
| Safety Statements | 26-36-24/25-37/39 | |||||||||
| WGK Germany | 3 | |||||||||
| RTECS | NL9500000 | |||||||||
| F | 8 | |||||||||
| Hazard Note | Irritant | |||||||||
| HazardClass | IRRITANT, KEEP COLD, LIGHT SENSITIVE | |||||||||
| HS Code | 29339900 | |||||||||
| NFPA 704 |
|
5-Methoxyindole price More Price(8)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich(India) | M14900 | 5-Methoxyindole 99% | 1006-94-6 | 1G | ₹2619.65 | 2022-06-14 | Buy |
| Sigma-Aldrich(India) | M14900 | 5-Methoxyindole 99% | 1006-94-6 | 5G | ₹8746.6 | 2022-06-14 | Buy |
| TCI Chemicals (India) | M0731 | 5-Methoxyindole min. 99.0 % | 1006-94-6 | 1G | ₹2100 | 2022-05-26 | Buy |
| TCI Chemicals (India) | M0731 | 5-Methoxyindole min. 99.0 % | 1006-94-6 | 5G | ₹5200 | 2022-05-26 | Buy |
| TCI Chemicals (India) | M0731 | 5-Methoxyindole min. 99.0 % | 1006-94-6 | 25G | ₹16000 | 2022-05-26 | Buy |
5-Methoxyindole Chemical Properties,Uses,Production
Chemical Properties
white to light brownish crystalline powder
Uses
5-Methoxyindole (cas# 1006-94-6) is a compound useful in organic synthesis. It can be used to synthesis 1-(Phenylsulfonyl)-5-methoxy-1H-indole.
Preparation
The synthesis of 5-methoxyindole from 5-methoxy-2-oxindole: Conversion of 5-methoxy-2-oxindole to 5-methoxyindole was accomplishedby the chlorination of 5-methoxy-2-oxindole with triphenylphosphine-carbontetrachloride in acetonitrile followed by the catalytic reduction of a chlorine atom in 66% total yield.
Reactions
5-methoxyindole was treated with sodium hydroxide and phenylsulfonyl chloride in the presence of a catalytic amount of tetrabutylammonium bromide to afford 1-(phenylsulfonyl)indole and 5-methoxy-1-(phenylsufonyl)indole in excellent yields of 100%.
Purification Methods
Crystallise 5-methoxyindole from cyclohexane pet ether or pet ether/Et2O. [Saito & Kikugawa J Heterocycl Chem 16 1325 1979, Beilstein 21 III/IV 765, 21/3 V 18.]
5-Methoxyindole Preparation Products And Raw materials
Raw materials
EthenaMine, 2-(5-Methoxy-2-nitrophenyl)-N,N-diMethyl-, (1E)-
1-Propanone, 1-(5-methoxy-1H-indol-1-yl)-2,2-dimethyl-
Benzene, 2-ethenyl-4-methoxy-1-nitro-
5-Methoxyindole-3-carboxaldehyde
Phosphonium, [2-(1,1-dimethylethoxy)-2-oxoethyl]triphenyl-, inner salt
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1006-94-6(5-Methoxyindole)Related Search:
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5-Methoxyindole ,98%
5-METHOXYINDOLE (5MeOI)
5-methoxy-1H-indole(SALTDATA: FREE)
5-MethoxyindoleF
5-METHOXYINDOLE REPANIDAL
NSC 521752
5-METHOXYINDOLE
AKOS JY2082918
RARECHEM AH BS 0117
TIMTEC-BB SBB004094
1H-Indol-5-yl methyl ether
Femedol
Indole, 5-methoxy-
Methoxy-5 indole
methoxy-5indole
5-Methyoxy Indole
5-methyloxyl indole
5-Methoxylindole
Methoxyindole,99%
Indol-5-yl methyl ether
5-Methoxyindole in stock Factory
5-Methoxyindole>
5-Methoxyindole 1006-94-6
Methoxyindole 99% indol-5-yl methyl ether
5-METHOXY-1H-INDOLE
5-methoxy-indol
1006-94-6
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