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N-Methylphthalimide

N-Methylphthalimide Structure
CAS No.
550-44-7
Chemical Name:
N-Methylphthalimide
Synonyms
2-Methylisoindoline-1,3-dione;T56 BVNVJ C1;METHYL PHTHALIMIDE;N-METHYLPHTHALIMIDE;n-methyl-phthalimid;PHTHALIMIDE-N-METHYL;N-Methylphthalimide>2-Methyl-1H-isoindole-1;N-Methylphthalimide,98%;Rivaroxaban Impurity 20
CBNumber:
CB8473039
Molecular Formula:
C9H7NO2
Molecular Weight:
161.16
MOL File:
550-44-7.mol
MSDS File:
SDS
Modify Date:
2023/4/27 16:27:43

N-Methylphthalimide Properties

Melting point 129-132 °C (lit.)
Boiling point 286.05°C
Density 1.2443 (rough estimate)
refractive index 1.4500 (estimate)
storage temp. Sealed in dry,Room Temperature
solubility DMSO (Slightly), Methanol (Slightly)
form Solid
pka -2.09±0.20(Predicted)
color White to Off-White
BRN 124428
CAS DataBase Reference 550-44-7(CAS DataBase Reference)
NIST Chemistry Reference 1H-Isoindole-1,3(2H)-dione, 2-methyl-(550-44-7)
EPA Substance Registry System 1H-Isoindole-1,3(2H)-dione, 2-methyl- (550-44-7)

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P264-P271-P280-P302+P352-P305+P351+P338
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-36
WGK Germany  1
RTECS  TI5602700
TSCA  Yes
HazardClass  IRRITANT
HS Code  29251900
NFPA 704
1
2 0

N-Methylphthalimide price More Price(2)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich(India) 407992 N-Methylphthalimide 98% 550-44-7 5G ₹3052.65 2022-06-14 Buy
TCI Chemicals (India) M0299 N-Methylphthalimide min. 99.0 % 550-44-7 25G ₹5200 2022-05-26 Buy
Product number Packaging Price Buy
407992 5G ₹3052.65 Buy
M0299 25G ₹5200 Buy

N-Methylphthalimide Chemical Properties,Uses,Production

Chemical Properties

White powder

Uses

Photoreduction of N-methylphthalimide (NMP) with 2,3-dimethyl-2-butene h and the selective electroreduction of N-methylphthalimide to 3-hydroxy-2-methyl-isoindolin-1-one have been studied.

General Description

Photoreduction of N-methylphthalimide (NMP) with 2,3-dimethyl-2-butene has been studied. The selective electroreduction of N-methylphthalimide to 3-hydroxy-2-methyl-isoindolin-1-one in ionic liquids and phenol as a proton donor under silent and ultrasonic conditions has been reported. Single electron transfer (SET)-induced photochemical reaction of NMP with silyl enol ether has been investigated. Nitration of NMP is reported to afford “exclusively” 3-nitro-derivative.

Purification Methods

Recrystallise the imide from absolute EtOH or AcOH (m 134o). The IR has max at 1780 and 1380cm -1. [Beilstein 21 H 461, 21 III/IV 5030.]

N-Methylphthalimide Preparation Products And Raw materials

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2-Methyl-1H-isoindole-1 Rivaroxaban Impurity F ( N-Methyl Phthalimide ) CAS No. 550-44-7 Imp. F:N-Methylphthalimide Rivaroxaban impurity P1-B 1H-Isoindole-1,3(2H)-dione,2-methyl- 2-Methyl-1H-isoindol-1,3(2H)-dion 2-methyl-1h-isoindole-3(2h)-dione 2-Methyl-isoindole-1,3-dione n-methyl-phthalimid N-METHYLPHTHALIMIDE PHTHALIMIDE-N-METHYL 2-METHYL-1H-ISOINDOLE-1,3(2H)-DIONE METHYL PHTHALIMIDE N-Methylphthalimide,98% n-methyl-1h-isoindole-1,3-(2h)-dione Rivaroxaban N-Methylphthalimide Impurity Rivaroxaban Impurity F ( N-Methyl Phthalimide ) Rivaroxaban Impurity 20 Rivaroxaban related mixture 1 (N-methyl collar phthalimide) N-Methylphthalimide> Rivaroxaban Impurity F/ Rivaroxaban N-Methylphthalimide Impurity T56 BVNVJ C1 2-Methylisoindoline-1,3-dione Rivaroxaban Impurity 99 (N-Methyl Phthalimide) 550-44-7 Carbonyl Compounds Building Blocks Cyclic Imides Organic Building Blocks N-Substituted Maleimides, Succinimides & Phthalimides N-Substituted Phthalimides intermediates N-Substituted Maleimides, Succinimides & Phthalimides N-Substituted Phthalimides Cyclic ImidesDerivatization Reagents Carbonyl Compounds Derivatization Reagents HPLC Organic Building Blocks UV-VIS API intermediates