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9-phenylanthracene

9-phenylanthracene Structure
CAS No.
602-55-1
Chemical Name:
9-phenylanthracene
Synonyms
NSC 90796;9-phenylantracene;9-PHENYLANTHRACENE;Phenylanthracene,98%;anthracene,9-phenyl-;9-Phenylanthracene97%;9-Phenylanthracene>9-Phenylanthracene,98%;9-Phenylanthracene 97%;9-PHENYLANTHRACENE OEKANAL
CBNumber:
CB8778824
Molecular Formula:
C20H14
Molecular Weight:
254.33
MOL File:
602-55-1.mol
MSDS File:
SDS
Modify Date:
2023/11/8 17:00:29
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9-phenylanthracene Properties

Melting point 153-155 °C (lit.)
Boiling point 417 °C (lit.)
Density 1.1180 (estimate)
refractive index 1.7040 (estimate)
storage temp. Sealed in dry,Room Temperature
solubility Chloroform (Slightly), Ethyl Acetate (Slightly)
form Solid
color Off-white to pale brown
Sensitive Light Sensitive
BRN 1910570
CAS DataBase Reference 602-55-1(CAS DataBase Reference)
EPA Substance Registry System Anthracene, 9-phenyl- (602-55-1)

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS09
Signal word  Warning
Hazard statements  H410
Precautionary statements  P273-P501
Hazard Codes  N
Risk Statements  50/53
Safety Statements  60-61
RIDADR  UN 3077 9/PG 3
WGK Germany  3
HazardClass  9
HS Code  29029090
NFPA 704
1
0 0

9-phenylanthracene price More Price(5)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich(India) P18004 9-Phenylanthracene 98% 602-55-1 1G ₹4233.3 2022-06-14 Buy
Sigma-Aldrich(India) P18004 9-Phenylanthracene 98% 602-55-1 5G ₹13819.88 2022-06-14 Buy
TCI Chemicals (India) P0138 9-Phenylanthracene min. 98.0 % 602-55-1 1G ₹2700 2022-05-26 Buy
TCI Chemicals (India) P0138 9-Phenylanthracene min. 98.0 % 602-55-1 5G ₹11100 2022-05-26 Buy
TCI Chemicals (India) P0138 9-Phenylanthracene min. 98.0 % 602-55-1 25G ₹45500 2022-05-26 Buy
Product number Packaging Price Buy
P18004 1G ₹4233.3 Buy
P18004 5G ₹13819.88 Buy
P0138 1G ₹2700 Buy
P0138 5G ₹11100 Buy
P0138 25G ₹45500 Buy

9-phenylanthracene Chemical Properties,Uses,Production

Chemical Properties

Pale Yellow Plates

Uses

9-Phenylanthracene is used to synthesize organic light-emitting material intermediates.

Preparation

The synthesis of 9-phenylanthracene involved mixing phenylboronic acid (2.13 g, 17.49 mmol), 9-bromoanthracene (3 g, 11.66 mmol), Pd(PPh3)4 (140 mg, 0.12 mmol), K2CO3 (16 mL, 2 M), and ethanol (8 mL) in a 100 mL flask with anhydrous toluene (32 mL). The mixture was refluxed for 48 h under nitrogen. After cooled to room temperature, the reaction mixture was quenched with dilute hydrochloric acid solution and extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation. The crude product was further purified by silica gel column chromatography (CH2Cl2/petroleum ether (1:4,v/v)) to get a white powder (2.43 g, 81.9 %). 1H NMR (500 MHz, CDCl3) δ 8.53 (s, 1H), 8.08 (d, J = 8.5 Hz, 2H), 7.70 – 7.67 (m, 2H), 7.63 – 7.54 (m, 3H), 7.50 – 7.45 (m, 4H), 7.37 (ddd, J = 8.7, 6.5, 1.2 Hz, 2H). EI-MS (m/z): Calculated for C20H14: 254.33. Found [M+]: 253.02.
preparation of 9-phenylanthracene
Synthesis of 9-phenylanthracene

Purification Methods

Chromatograph it on alumina in *C6H6 and recrystallise it from AcOH or toluene. [Beilstein 5 H 725, 5 II 639, 5 III 2462.]

9-phenylanthracene Preparation Products And Raw materials

Raw materials

Anthrone Bromobenzene Magnesium Phenylboronic acid 9-Bromoanthracene
Tetrakis(triphenylphosphine)palladium Potassium carbonate Ethanol
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Preparation Products

9-phenylanthracene Suppliers

Global( 176)Suppliers
Supplier Tel Country ProdList Advantage Inquiry
ORGANO FINE CHEMICALS +91-91-22-42128300 +91-2242128300 Mumbai, India 258 58 Inquiry
TCI Chemicals (India) Pvt. Ltd. 1800 425 7889 New Delhi, India 6778 58 Inquiry
CLEARSYNTH LABS LTD. +91-22-45045900 Hyderabad, India 6351 58 Inquiry
A.J Chemicals 91-9810153283 New Delhi, India 6124 58 Inquiry
Organo Fine Chemicals +91 (22) 2201-6968 / 2206-7521 New Delhi, India 266 60 Inquiry
Hebei Xinsheng New Material Technology Co., LTD. +86-16632316109 China 1092 58 Inquiry
Springchem New Material Technology Co.,Limited +86-021-62885108 +8613917661608 China 2068 57 Inquiry
Shanghai Daken Advanced Materials Co.,Ltd +86-371-66670886 China 16209 58 Inquiry
ATK CHEMICAL COMPANY LIMITED +undefined-21-51877795 China 32760 60 Inquiry
career henan chemical co +86-0371-86658258 +8613203830695 China 29900 58 Inquiry
Supplier Advantage
ORGANO FINE CHEMICALS 58
TCI Chemicals (India) Pvt. Ltd. 58
CLEARSYNTH LABS LTD. 58
A.J Chemicals 58
Organo Fine Chemicals 60
Hebei Xinsheng New Material Technology Co., LTD. 58
Springchem New Material Technology Co.,Limited 57
Shanghai Daken Advanced Materials Co.,Ltd 58
ATK CHEMICAL COMPANY LIMITED 60
career henan chemical co 58

9-phenylanthracene Spectrum

9-phenylanthracene(602-55-1)MS9-phenylanthracene(602-55-1)1HNMR9-phenylanthracene(602-55-1)13CNMR9-phenylanthracene(602-55-1)IR19-phenylanthracene(602-55-1)IR29-phenylanthracene(602-55-1)Raman

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