Amisulpride synthesis
- Product Name:Amisulpride
- CAS Number:71675-85-9
- Molecular formula:C17H27N3O4S
- Molecular Weight:369.48
26116-12-1
377 suppliers
$6.00/5g
541-41-3
6 suppliers
$21.00/5g
71675-85-9
516 suppliers
$39.00/25mg
Yield:71675-85-9 100%
Reaction Conditions:
in triethylamine;acetone;
Steps:
V Levorotatory N-[1-ethyl 2-pyrrolidylmethyl] 2-methoxy 4-amino 5-ethylsulphonyl benzamide
Levorotatory N-[1-ethyl 2-pyrrolidylmethyl] 2-methoxy 4-amino 5-ethylsulphonyl benzamide Following the same procedure as in Example I, 104 g of 2-methoxy 4-amino 5-ethylsulphonyl benzoic acid dissolved in 380 ml of acetone, in the presence of 38 g of triethylamine, is treated with 41 g of ethyl chloroformate then with 58 g of levorotatory 1-ethyl 2-aminomethyl pyrrolidine. 140 g of levorotatory N[1-ethyl 2-pyrrolidylmethyl] 2-methoxy 4-amino 5-ethylsulphonyl benzamide is obtained (yield 100%).
References:
US4294828,1981,A
26116-12-1
377 suppliers
$6.00/5g
71675-87-1
375 suppliers
$10.00/1g
71675-85-9
516 suppliers
$39.00/25mg
26116-12-1
377 suppliers
$6.00/5g
71675-87-1
375 suppliers
$10.00/1g
541-41-3
6 suppliers
$21.00/5g
71675-85-9
516 suppliers
$39.00/25mg
74-96-4
439 suppliers
$9.00/5g
176849-91-5
44 suppliers
inquiry
71675-85-9
516 suppliers
$39.00/25mg
27492-84-8
316 suppliers
$6.00/5g
71675-85-9
516 suppliers
$39.00/25mg