2-Chloro-N,N-dimethylacetamide
- CAS No.
- 2675-89-0
- Chemical Name:
- 2-Chloro-N,N-dimethylacetamide
- Synonyms
- EOS-61825;AKOS BBS-00000943;2-Chloro-N,N-dimethy;CHLOROACETYLDIMETHYLAMINE;N,N-DIMETHYLCHOROACETAMIDE;N,N-DIMETHYLCHLOROACETAMIDE;N-DiMethyl-2-chloroacetaMide;N,N-DIMETHYL-2-CHLOROACETAMIDE;2-CHLORO-N,N-DIMETHYLACETAMIDE;2-CHLORO-N,N-DIMETHYL ACETAMINE
- CBNumber:
- CB2343589
- Molecular Formula:
- C4H8ClNO
- Molecular Weight:
- 121.57
- MOL File:
- 2675-89-0.mol
- MSDS File:
- SDS
- Modify Date:
- 2023/4/23 13:52:06
| Melting point | 15-16 °C |
|---|---|
| Boiling point | 98-100°C/11mm |
| Density | 1.182 g/mL at 20 °C (lit.) |
| refractive index |
n |
| Flash point | 98-100°C/11mm |
| storage temp. | Store below +30°C. |
| solubility | Chloroform (Slightly), Hexane (Slightly), Methanol (Slightly) |
| pka | -0.95±0.70(Predicted) |
| form | Liquid |
| color | Clear colorless to pale yellow |
| BRN | 969568 |
| InChIKey | XBPPLECAZBTMMK-UHFFFAOYSA-N |
| CAS DataBase Reference | 2675-89-0(CAS DataBase Reference) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |   GHS05,GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Danger | |||||||||
| Hazard statements | H302-H314 | |||||||||
| Precautionary statements | P270-P280-P301+P312-P303+P361+P353-P304+P340+P310-P305+P351+P338 | |||||||||
| Hazard Codes | C | |||||||||
| Risk Statements | 22-34 | |||||||||
| Safety Statements | 26-36/37/39-45 | |||||||||
| RIDADR | UN 3265 8/PG 3 | |||||||||
| WGK Germany | 3 | |||||||||
| HS Code | 29241990 | |||||||||
| NFPA 704 |
|
2-Chloro-N,N-dimethylacetamide price More Price(6)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich(India) | 24350 | 2-Chloro-N,N-dimethylacetamide ≥97.0% (GC) | 2675-89-0 | 25ML | ₹23620.15 | 2022-06-14 | Buy |
| TCI Chemicals (India) | C3011 | 2-Chloro-N,N-dimethylacetamide min. 97.0 % | 2675-89-0 | 5G | ₹2100 | 2022-05-26 | Buy |
| ALFA India | ALF-H50229-MD | 2-Chloro-N,N-dimethylacetamide, 97% | 2675-89-0 | 250mg | ₹10372 | 2022-05-26 | Buy |
| TCI Chemicals (India) | C3011 | 2-Chloro-N,N-dimethylacetamide min. 97.0 % | 2675-89-0 | 25G | ₹6100 | 2022-05-26 | Buy |
| ALFA India | ALF-H50229-06 | 2-Chloro-N,N-dimethylacetamide, 97% | 2675-89-0 | 1ea | ₹9202 | 2022-05-26 | Buy |
2-Chloro-N,N-dimethylacetamide Chemical Properties,Uses,Production
Uses
2-Chloro-N,N-dimethylacetamide is N,M-dialkyl amide used as an organic catalyst in the preparation of phosphorylated thiosemicarbazide.
Synthesis
In a 500 mL four-necked flask, sodium hydrogen carbonate 126.0 g (1.50 mol) and 146.8 g of toluene were added, and the mixture was stirred while cooling. The internal temperature was maintained below 5 ° C, 112.9 g (1.00 mol) of chloroacetyl chloride was added dropwise over 4 hours, and 49.6 g (1.10 mol) of dimethylamine gas was blown over 4 hours. After stirring at -2 to 1 ° C. for 1 hour, the reaction solution was filtrated under reduced pressure to remove inorganic salt crystals by filtration. The crystals were washed with 100 g of toluene, and the filtrate and washings were combined. After separating and removing the aqueous layer in the filtrate washings, the toluene layer was concentrated under reduced pressure to obtain 113.2 g (0.93 mol) of oily 2-chloro-N, N-dimethylacetamide. The yield was 93.1%.
2-Chloro-N,N-dimethylacetamide Preparation Products And Raw materials
Raw materials
1of2
chevron_rightPreparation Products
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| A.R. LIFE SCIENCES PVT. LTD. | +91-914040267679 +91-8519993257 | Hyderabad, India | 100 | 58 | Inquiry |
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| TCI Chemicals (India) Pvt. Ltd. | 1800 425 7889 | New Delhi, India | 6778 | 58 | Inquiry |
| Alfa Aesar | 1 800 209 7001 | Maharashtra, India | 6913 | 58 | Inquiry |
| Manus Aktteva Biopharma LLP | 08048250218Ext 800 | Ahmedabad, India | 655 | 58 | Inquiry |