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ChemicalBook CAS DataBase List TRANS-3-DECENE

TRANS-3-DECENE synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 93 percent / NaH / 1.) THF, 2.) HMPA, -20 deg C to room temp. then room temp., overnight
2: 16.3 percent Chromat. / Na, liquid NH3 / tetrahydrofuran / 2 h / Heating

References:

Doolittle, Robert E.;Patrick, Delrea G.;Heath, Robert H. [Journal of Organic Chemistry,1993,vol. 58,# 19,p. 5063 - 5066]

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