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1-Propanesulfonyl chloride

1-Propanesulfonyl chloride  Structure
CAS No.
10147-36-1
Chemical Name:
1-Propanesulfonyl chloride
Synonyms
PROPANE-1-SULFONYL CHLORIDE;Tirofiban Impurity 73;Propyl sulfonyl chloride;propanesulphonyl chloride;PROPANE SULFONYL CHLORIDE;1-PROPANESULFONYL CHLORIDE;1-PropanesulfonylChloride>1-Propanesulfonyl chloride,99%;1-Propanesulfonyl chloride 97%;Propanesulphonyl chloride,>98%
CBNumber:
CB8374668
Molecular Formula:
C3H7ClO2S
Molecular Weight:
142.6
MOL File:
10147-36-1.mol
Modify Date:
2024/8/24 19:19:26

1-Propanesulfonyl chloride Properties

Melting point -37 °C
Boiling point 78-79 °C/15 mmHg (lit.)
Density 1.267 g/mL at 25 °C (lit.)
vapor density 4.9 (vs air)
refractive index n20/D 1.453(lit.)
Flash point 176 °F
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
form clear liquid
color Colorless to Light yellow
Water Solubility Decomposes in hot water.
Sensitive Moisture Sensitive
BRN 1747500
CAS DataBase Reference 10147-36-1(CAS DataBase Reference)
NIST Chemistry Reference 1-Propanesulfonyl chloride(10147-36-1)
EPA Substance Registry System 1-Propanesulfonyl chloride (10147-36-1)

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS05
Signal word  Danger
Hazard statements  H314
Precautionary statements  P280-P303+P361+P353-P304+P340+P310-P305+P351+P338-P337+P313-P363
Hazard Codes  C
Risk Statements  14-34-36-R36-R34-R14
Safety Statements  26-36/37/39-45-S45-S36/37/39-S26
RIDADR  UN 3265 8/PG 2
WGK Germany  3
10-19-21
TSCA  Yes
HazardClass  8
PackingGroup  III
HS Code  29049090
NFPA 704
1
3 2
W

1-Propanesulfonyl chloride price More Price(3)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 303771 1-Propanesulfonyl chloride 97% 10147-36-1 100ML ₹12923.75 2022-06-14 Buy
Sigma-Aldrich(India) 303771 1-Propanesulfonyl chloride 97% 10147-36-1 100ML ₹12923.75 2022-06-14 Buy
TCI Chemicals (India) P0693 1-Propanesulfonyl Chloride min. 98.0 % 10147-36-1 25G ₹13900 2022-05-26 Buy
Product number Packaging Price Buy
303771 100ML ₹12923.75 Buy
303771 100ML ₹12923.75 Buy
P0693 25G ₹13900 Buy

1-Propanesulfonyl chloride Chemical Properties,Uses,Production

Chemical Properties

Light yellow liquid

Uses

1-Propanesulfonyl chloride was used in synthesis of 1-alkyl-3-methylimidazolium alkanesulfonate ionic liquids.

Synthesis

2,4,6-Trichloro-[1,3,5]-triazine (TCT) was added at room temperature to a solution of propane-1-sulfonic acid in acetone dry, followed by NEt3 dropwise. The resulting mixture was irradiated to 80 °C (50 W of MW power) for 20 min in a sealed tube (10 mL pressure-rated reaction vial) in a self-tuning single-mode irradiating synthesizer. The mixture was cooled rapidly to room temperature by passing compressed air through the microwave cavity for 1 min. After cooling to room temperature, the precipitate was filtered off on Celite to afford 1-Propanesulfonyl chloride[1].
1-Propanesulfonyl chloride

References

[1] Lidia De Luca, Giampaolo Giacomelli. “An Easy Microwave-Assisted Synthesis of Sulfonamides Directly from Sulfonic Acids.” The Journal of Organic Chemistry 73 10 (2008): 3967–3969.

1-Propanesulfonyl chloride Preparation Products And Raw materials

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