1-Methyl-3-pyrrolidinol
- CAS No.
- 13220-33-2
- Chemical Name:
- 1-Methyl-3-pyrrolidinol
- Synonyms
- 1-METHYL-PYRROLIDIN-3-OL;3-HYDROXY-1-METHYLPYRROLIDINE;NSC 89279;3-Hydroxy-1-methyL;N-Methyl-3-hydroxy-;1-Methyl-3-pyrrolidi;N-methyl-3-pyrrolitol;N-Methyl-3-pyrrolidinol;1-METHYL-3-PYRROLIDINOL;N-Methyl-pyrrolidin-3-ol
- CBNumber:
- CB9296691
- Molecular Formula:
- C5H11NO
- Molecular Weight:
- 101.15
- MOL File:
- 13220-33-2.mol
- MSDS File:
- SDS
- Modify Date:
- 2024/4/24 19:16:04
| Boiling point | 50-52 °C1 mm Hg(lit.) |
|---|---|
| Density | 0.921 g/mL at 25 °C(lit.) |
| refractive index |
n |
| Flash point | 159 °F |
| storage temp. | 2-8°C |
| solubility | Chloroform (Slightly), Methanol (Slightly) |
| form | Oil |
| pka | 14.95±0.20(Predicted) |
| color | Colourless |
| InChI | InChI=1S/C5H11NO/c1-6-3-2-5(7)4-6/h5,7H,2-4H2,1H3 |
| InChIKey | FLVFPAIGVBQGET-UHFFFAOYSA-N |
| SMILES | N1(C)CCC(O)C1 |
| CAS DataBase Reference | 13220-33-2(CAS DataBase Reference) |
| NIST Chemistry Reference | 1-Methyl-3-pyrrolidinol(13220-33-2) |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|||||||||
|---|---|---|---|---|---|---|---|---|---|---|
| Signal word | Warning | |||||||||
| Hazard statements | H227-H315-H319-H335 | |||||||||
| Precautionary statements | P210e-P261-P280a-P305+P351+P338-P405-P501a | |||||||||
| Hazard Codes | Xi | |||||||||
| Risk Statements | 36/37/38 | |||||||||
| Safety Statements | 26-36/37/39 | |||||||||
| WGK Germany | 3 | |||||||||
| HS Code | 29339900 | |||||||||
| NFPA 704 |
|
1-Methyl-3-pyrrolidinol price More Price(4)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich(India) | M79506 | 1-Methyl-3-pyrrolidinol 95% | 13220-33-2 | 1G | ₹17330.83 | 2022-06-14 | Buy |
| Sigma-Aldrich(India) | M79506 | 1-Methyl-3-pyrrolidinol 95% | 13220-33-2 | 5G | ₹66811.9 | 2022-06-14 | Buy |
| TCI Chemicals (India) | M2115 | 1-Methyl-3-pyrrolidinol min. 97.0 % | 13220-33-2 | 5G | ₹8600 | 2022-05-26 | Buy |
| TCI Chemicals (India) | M2115 | 1-Methyl-3-pyrrolidinol min. 97.0 % | 13220-33-2 | 25G | ₹29200 | 2022-05-26 | Buy |
1-Methyl-3-pyrrolidinol Chemical Properties,Uses,Production
Chemical Properties
Clear colorless to pale yellow liquid
Uses
1-Methyl-3-pyrrolidinol (cas# 13220-33-2) is a compound useful in organic synthesis.
Synthesis
A 500 mL four-necked flask was charged with a 40 wt% aqueous solution of monomethylamine and cooled to 10 ° C in an ice-water bath. Then, while stirring, 1,4-dichloro-2-butanol was added dropwise, and the temperature was controlled at 15 ° C. Then pour the system into an Autoclave, sealed, evacuated to a pressure of 1.0 ± 0.1MPa, while heated to 120 ℃, the reaction was stirred for about 10h. After the reaction was over and cooled to room temperature, the material was discharged, batch-wise added sodium hydroxide was released, and a large amount of methylamine gas, controlling the temperature below 50 ℃, precipitated a lot of white solid, stirred for 1h; filtration, the filtrate layered, the upper organic phase Ethanol And anhydrous magnesium sulfate, stirring 2 ~ 3h; and then filtered, the filtrate was concentrated in vacuo to give a yellow transparent oily liquid, and then vacuum distillation to give colorless and t1-Methyl-3-pyrrolidinol, Yield 64.8%, purity 99.3%.
1-Methyl-3-pyrrolidinol Preparation Products And Raw materials
Raw materials
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chevron_rightPreparation Products
| Supplier | Tel | Country | ProdList | Advantage | Inquiry |
|---|---|---|---|---|---|
| BTC pharm India | +918790379245 | AndhraPradesh, India | 1269 | 58 | Inquiry |
| CLEARSYNTH LABS LTD. | +91-22-45045900 | Mumbai, India | 66 | 58 | Inquiry |
| NILKANTH HEALTH CHEM (I) PRIVATE LIMITED | +91 8000452862 | Gujarat, India | 17 | 58 | Inquiry |
| RESONANCE LABS | +91-8027630180 +91-8027630180 | Karnataka, India | 32 | 58 | Inquiry |
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| Alkaloids Private Limited | +91-9866110664 +91-9866110664 | Telangana, India | 25 | 58 | Inquiry |
| CHEMAZON LABORATORIES | +91 9848551964 | Hyderabad, India | 1320 | 58 | Inquiry |
| Equilife Laboratories Pvt Ltd | +91-8007935656 +91-9822319778 | Maharashtra, India | 29 | 58 | Inquiry |
| TCI Chemicals (India) Pvt. Ltd. | 1800 425 7889 | New Delhi, India | 6778 | 58 | Inquiry |
| Alfa Aesar | 1 800 209 7001 | Maharashtra, India | 6913 | 58 | Inquiry |
| Supplier | Advantage |
|---|---|
| BTC pharm India | 58 |
| CLEARSYNTH LABS LTD. | 58 |
| NILKANTH HEALTH CHEM (I) PRIVATE LIMITED | 58 |
| RESONANCE LABS | 58 |
| GLP Pharma Standards | 58 |
| Alkaloids Private Limited | 58 |
| CHEMAZON LABORATORIES | 58 |
| Equilife Laboratories Pvt Ltd | 58 |
| TCI Chemicals (India) Pvt. Ltd. | 58 |
| Alfa Aesar | 58 |
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