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ChemicalBook > Product Catalog >Organic Chemistry >Carboxylic acids and derivatives >Ethyl 4-bromoacetoacetate

Ethyl 4-bromoacetoacetate

Ethyl 4-bromoacetoacetate Structure
CAS No.
13176-46-0
Chemical Name:
Ethyl 4-bromoacetoacetate
Synonyms
Ethyl 4-bromo-3-oxobutanoate;1KG,5KG;Ethyl 4-Vromoacetoacetate;Ethyl 4-bromoacetoacetate;4-broMo ethyl acetoacetate;Ethyl 4-bromo-3-oxo-butyrate;4-BroMoacetoacetic acid ethyl ester;4-Bromo-3-oxobutanoic acid Et ester;4-Bromo-3-oxo-butyric acid ethyl ester;4-BroMo-3-oxo-butyric acid Methyl ester
CBNumber:
CB9874938
Molecular Formula:
C6H9BrO3
Molecular Weight:
209.04
MOL File:
13176-46-0.mol
MSDS File:
SDS
Modify Date:
2024/7/30 14:17:11
Request For Quotation

Ethyl 4-bromoacetoacetate Properties

Boiling point 231.6 °C
Density 1.511
refractive index 1.5281 (estimate)
storage temp. 2-8°C(protect from light)
pka 9.56±0.46(Predicted)
form liquid
color Colourless

SAFETY

Risk and Safety Statements

Symbol(GHS) 
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P271-P280
Hazard Codes  F
HS Code  2918300090

Ethyl 4-bromoacetoacetate Chemical Properties,Uses,Production

Synthesis

To a solution of Ethyl acetoacetate (10.0 g, 76.9 mmol, 1 .0 eq) in acetic acid (30 mL) was added bromine (12.3 g, 76.9 mmol, 1 .0 eq) at 0 °C over 10 min. The mixture was stirred at 0 °C for 1 h, the solvent was removed under reduced pressure, and the residue was diluted with water (50 mL). The aqueous mixture was extracted with CH2CI2 (50 mL x 3). The combined organic layers were washed with brine (60 mL x 2), dried over MgS04 and concentrated under reduced pressure to give ethyl 4-bromo-3-oxobutanoate (14.3 g, 85 per cent) as a yellow oil.

Ethyl 4-bromoacetoacetate Preparation Products And Raw materials

Raw materials

Preparation Products

Diethyl succinosuccinate 4-Thiazoleacetic acid, ethyl ester (2-PHENYL-THIAZOL-4-YL)-ACETIC ACID Ethyl 4-(benzyloxy)-3-oxobutanoate methyl 4-bromo-3-oxo-butanoate
Imidazo[1,2-a]pyrimidin-2-yl-acetic acidethylester Butanoic acid, 4-(ethylthio)-3-oxo-, ethyl ester ethyl 3-oxo-4-(1,1,3-trioxo-2,3-dihydro-1,2-benzothiazol-2-yl)butanoate
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Ethyl 4-bromoacetoacetate Suppliers

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GLR Innovations 58
SYNIX LABS 58
ALS INDIA LIFE SCIENCES 58
COMBIOTECH PVT LTD 58
Pharma Affiliates 58
A.J Chemicals 58
Pharmaffiliates Analytics and Synthetics P. Ltd 58
Hebei Guanlang Biotechnology Co,.LTD 58
Speranza Chemical Co., Ltd. 55
career henan chemical co 58

13176-46-0(Ethyl 4-bromoacetoacetate)Related Search:

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4-BroMo-3-oxo-butyric acid Methyl ester 4-Bromo-3-oxo-butyric acid ethyl ester Ethyl 4-bromoacetoacetate 4-Bromo-3-oxobutanoic acid Et ester 4-broMo ethyl acetoacetate 4-BroMoacetoacetic acid ethyl ester 1KG,5KG Ethyl 4-Vromoacetoacetate Butanoic acid, 4-bromo-3-oxo-, ethyl ester Ethyl 4-bromo-3-oxobutanoate Ethyl 4-bromo-3-oxo-butyrate 13176-46-0 17780-81-7 Small molecule