1,5-Diphenylcarbazide
- CAS No.
- 140-22-7
- Chemical Name:
- 1,5-Diphenylcarbazide
- Synonyms
- DIPHENYLCARBAZIDE;dianilinourea;Diphenylcartazide;1,3-dianilinourea;BIPHENYL CARBAZIDE;TIMTEC-BB SBB008713;S-DIPHENYLCARBAZIDE;DiphenylCarbazideGr;1,5-Diphenylcarbazid;1,5-DIPHENYLCARBAZIDE
- CBNumber:
- CB9266061
- Molecular Formula:
- C13H14N4O
- Molecular Weight:
- 242.28
- MOL File:
- 140-22-7.mol
- MSDS File:
- SDS
- Modify Date:
- 2023/5/4 17:34:33
Melting point | 170-175 °C(lit.) |
---|---|
Boiling point | 385.1°C (rough estimate) |
Density | 1.31 g/cm3 |
refractive index | 1.6120 (estimate) |
storage temp. | 2-8°C |
solubility | aqueous acetone: passes test |
form | Powder or Flakes |
pka | 9.98±0.43(Predicted) |
color | White to cream |
Odor | Odorless |
Water Solubility | Soluble in glacial acetic acid, alcohol and acetone. Slightly soluble in water. |
Sensitive | Light Sensitive |
Merck | 14,3321 |
BRN | 752039 |
Stability | Stable. Light sensitive. Incompatible with strong oxidizing agents. |
CAS DataBase Reference | 140-22-7(CAS DataBase Reference) |
NIST Chemistry Reference | N'',n'''-diphenylcarbonohydrazide(140-22-7) |
EPA Substance Registry System | Carbonic dihydrazide, 2,2'-diphenyl- (140-22-7) |
SAFETY
Risk and Safety Statements
Symbol(GHS) | GHS07 |
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Signal word | Warning | |||||||||
Hazard statements | H315-H319 | |||||||||
Precautionary statements | P264-P280-P302+P352-P305+P351+P338-P332+P313-P337+P313 | |||||||||
Hazard Codes | Xi | |||||||||
Risk Statements | 36/37/38 | |||||||||
Safety Statements | 26-36 | |||||||||
WGK Germany | 3 | |||||||||
RTECS | FF2750000 | |||||||||
F | 8-10-23 | |||||||||
TSCA | Yes | |||||||||
HazardClass | IRRITANT | |||||||||
HS Code | 29280090 | |||||||||
NFPA 704 |
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1,5-Diphenylcarbazide price More Price(25)
Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
---|---|---|---|---|---|---|---|
Sigma-Aldrich(India) | D7766 | 1,5-Diphenylcarbazide reagent grade | 140-22-7 | 10G | ₹5845.5 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | D7766 | 1,5-Diphenylcarbazide reagent grade | 140-22-7 | 25G | ₹9060.53 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | D7766 | 1,5-Diphenylcarbazide reagent grade | 140-22-7 | 100G | ₹11474.5 | 2022-06-14 | Buy |
Sigma-Aldrich | 33152 | 1,5-Diphenylcarbazide reag. Ph. Eur., ≥98.0%, for metal titration | 140-22-7 | 10G | ₹5293.43 | 2022-06-14 | Buy |
Sigma-Aldrich(India) | 33152 | 1,5-Diphenylcarbazide reag. Ph. Eur., ≥98.0%, for metal titration | 140-22-7 | 10G | ₹5293.43 | 2022-06-14 | Buy |
1,5-Diphenylcarbazide Chemical Properties,Uses,Production
Chemical Properties
white crystals or powder
Uses
1,5-Diphenylcarbazideis a carbazide derivative used in the colorimteric determination of chromium as well as in the detection of cadmium, mercury, magnesium and aldehydes.
General Description
1,5-Diphenylcarbazide is a colorimetric reagent commonly employed in the determination of trace metals.
Purification Methods
A common impurity is phenyl-semicarbazide which can be removed by chromatography: ~8g in H2O is placed on a column (polyamide 6 powder, Macherey-Nagel-GmbH-Germany, washed several times with MeOH), eluted with H2O/MeOH/AcOH (1:3:0.04) at 7-8 drops/second, then eluted with the same solvent mixture but diluted 5 fold with H2O. The purification is followed by UV light at 280nm. The effluent is evaporated to dryness in vacuo at ~28o. [chromatography, IR & UV: Willems et al. Anal Chim Acta 51 544 1970]. Recrystallise it from EtOH by adding CCl4 to induce crystallisation, or AcOH to give a white crystalline powder which turns pink in air. It is air and light sensitive and should be stored in the dark under N2. [Beilstein 15 H 292, 15 IV 182.]
1,5-Diphenylcarbazide Preparation Products And Raw materials
Raw materials
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